5HWT
Crystal structure of apo-PAS1
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 173 |
Detector technology | CCD |
Collection date | 2012-07-06 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1 |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 41.114, 49.314, 56.222 |
格子定数 [度] | 90.00, 109.22, 90.00 |
精密化法
残基 | 25.000 - 1.700 |
R因子 | 0.1535 |
Rwork | 0.150 |
R-free | 0.22395 |
Structure solution method | MOLECULAR REPLACEMENT |
結合長の平均二乗偏差(RMSD) [Å] | 0.022 |
結合角の平均二乗偏差(RMSD) [度] | 2.039 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0049) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 1.730 |
分解能 [Å] (高) | 1.700 | 1.700 |
独立反射数 | 23475 | |
<I/σ(I)> | 32.94 | |
完全性 [%] | 100.0 | |
冗長性 | 7.4 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 294.15 | 3.0M ammonium phosphate, 0.1M Tris-HCl |