5FXY
Structure of the human RBBP4:MTA1(464-546) complex
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-07-24 |
Detector | DECTRIS PIXEL |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 81.294, 150.072, 95.591 |
格子定数 [度] | 90.00, 94.54, 90.00 |
精密化法
残基 | 95.290 - 3.200 |
R因子 | 0.25114 |
Rwork | 0.249 |
R-free | 0.29084 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4pc0 |
結合長の平均二乗偏差(RMSD) [Å] | 0.007 |
結合角の平均二乗偏差(RMSD) [度] | 1.053 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0135) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 95.300 | 3.340 |
分解能 [Å] (高) | 3.200 | 3.200 |
Rmerge_l_obs | 0.160 | 0.800 |
独立反射数 | 35054 | |
<I/σ(I)> | 5.3 | 2 |
完全性 [%] | 97.7 | 98 |
冗長性 | 4.2 | 4.2 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | 7.5 | 0.21 M AMMONIUM CITRATE AND 19% PEG 3350, pH 7.5 |