Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

5F31

Crystal structure of membrane associated PatA from Mycobacterium smegmatis in complex with palmitate - P 42 21 2 space group

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X10SA
Synchrotron siteSLS
BeamlineX10SA
Temperature [K]100
Detector technologyPIXEL
Collection date2011-12-19
DetectorDECTRIS PILATUS 6M
Wavelength(s)0.99996
Spacegroup nameP 42 21 2
Unit cell lengths80.302, 80.302, 113.766
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution40.187 - 2.430
R-factor0.2266
Rwork0.224
R-free0.27930
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.003
RMSD bond angle0.755
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHASER
Refinement softwarePHENIX (1.8.2_1309)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]40.190
High resolution limit [Å]2.4302.430
Rmerge0.1220.669
Number of reflections14652
<I/σ(I)>4.61.1
Completeness [%]100.0100
Redundancy10.510.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP8.5291100 mM Tris-HCl pH 8.5 and 20% ethanol

217705

건을2024-03-27부터공개중

PDB statisticsPDBj update infoContact PDBjnumon