5ANR
Structure of a human 4E-T - DDX6 - CNOT1 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-10-26 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 93.129, 93.129, 175.329 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.324 - 2.102 |
R-factor | 0.195 |
Rwork | 0.193 |
R-free | 0.23190 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ct4 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.035 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.320 | 2.180 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.090 | 1.040 |
Number of reflections | 51910 | |
<I/σ(I)> | 17.61 | 1.6 |
Completeness [%] | 99.7 | 97.4 |
Redundancy | 9.4 | 7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 8 | 50 MM TRIS PH 8.0, 35% MPD |