Experimental procedure
| Source type | ROTATING ANODE |
| Source details | ELLIOTT GX-21 |
| Temperature [K] | 290 |
| Detector technology | FILM |
| Detector | FILM |
| Spacegroup name | H 3 2 |
| Unit cell lengths | 91.600, 91.600, 268.500 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 20.000 - 2.300 |
| R-factor | 0.193 * |
| Rwork | 0.193 |
| Structure solution method | MIR |
| RMSD bond length | 0.019 |
| RMSD bond angle | 19.578 * |
| Data reduction software | OSCTST |
| Data scaling software | CCP4 ((ROTAVATA)) |
| Phasing software | NEWREF ((LYNN TEN EYCK)) |
| Refinement software | TNT (1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 2.300 |
| Rmerge | 0.096 |
| Number of reflections | 17141 |
| Completeness [%] | 84.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Microdialysis * | 7.5 | or batch * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | ammonium sulfate | 42 (%sat) | |
| 2 | 1 | 1 | phosphate | 1.2 (M) |
