4W6R
Crystal Structure of Full-Length Split GFP Mutant D102C Disulfide Dimer, P 1 Space Group
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-06-08 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9792 |
Spacegroup name | P 1 |
格子定数 [Å] | 92.420, 92.560, 124.530 |
格子定数 [度] | 94.94, 96.17, 102.25 |
精密化法
残基 | 89.880 - 3.471 |
R因子 | 0.312 |
Rwork | 0.307 |
R-free | 0.35700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2b3p |
結合長の平均二乗偏差(RMSD) [Å] | 0.010 |
結合角の平均二乗偏差(RMSD) [度] | 1.841 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE: DEV_1555)) |
Quality characteristics
Overall | |
分解能 [Å] (低) | 89.880 |
分解能 [Å] (高) | 3.471 |
独立反射数 | 46082 |
<I/σ(I)> | 5.7 |
完全性 [%] | 89.4 |
冗長性 | 1.9 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 20% PEG3350, 0.2M NaSCN |