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4UO6

Structure of the A_Canine_Colorado_17864_06 H3 haemagglutinin in complex with Sialyl Lewis X

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I02
Synchrotron siteDiamond
BeamlineI02
Temperature [K]100
Detector technologyPIXEL
DetectorDECTRIS PILATUS 2M
Spacegroup nameP 63 2 2
Unit cell lengths96.926, 96.926, 349.576
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution174.790 - 2.900
R-factor0.19001
Rwork0.188
R-free0.23451
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4uo4
RMSD bond length0.007
RMSD bond angle1.249
Data reduction softwareXDS
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0069)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]48.4603.060
High resolution limit [Å]2.9002.900
Rmerge0.1000.650
Number of reflections22519
<I/σ(I)>17.62.3
Completeness [%]99.699.6
Redundancy8.99.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1

217705

건을2024-03-27부터공개중

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