4UO6
Structure of the A_Canine_Colorado_17864_06 H3 haemagglutinin in complex with Sialyl Lewis X
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 2M |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 96.926, 96.926, 349.576 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 174.790 - 2.900 |
R-factor | 0.19001 |
Rwork | 0.188 |
R-free | 0.23451 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4uo4 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.249 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.460 | 3.060 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.100 | 0.650 |
Number of reflections | 22519 | |
<I/σ(I)> | 17.6 | 2.3 |
Completeness [%] | 99.6 | 99.6 |
Redundancy | 8.9 | 9.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |