4UJ7
Structure of the S-layer protein SbsC, domains 5-6
Experimental procedure
| 実験手法 | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 1 21 1 |
| 格子定数 [Å] | 49.096, 43.753, 49.715 |
| 格子定数 [度] | 90.00, 103.78, 90.00 |
精密化法
| 残基 | 48.280 - 1.540 |
| R因子 | 0.19121 |
| Rwork | 0.190 |
| R-free | 0.21665 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4iuc |
| 結合長の平均二乗偏差(RMSD) [Å] | 0.008 |
| 結合角の平均二乗偏差(RMSD) [度] | 1.242 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.6.0117) |
Quality characteristics
| Overall | Outer shell | |
| 分解能 [Å] (低) | 48.300 | 1.640 |
| 分解能 [Å] (高) | 1.540 | 1.540 |
| Rmerge_l_obs | 0.040 | 0.290 |
| 独立反射数 | 30189 | |
| <I/σ(I)> | 15.7 | 3 |
| 完全性 [%] | 98.8 | 95.7 |
| 冗長性 | 3.4 | 3.1 |
結晶化条件
| 結晶ID | 方法 | pH | 温度 | 溶液条件 |
| 1 |
