4TU0
CRYSTAL STRUCTURE OF CHIKUNGUNYA VIRUS NSP3 MACRO DOMAIN IN COMPLEX WITH A 2'-5' OLIGOADENYLATE TRIMER
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2008-11-13 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.86 |
Spacegroup name | P 31 |
格子定数 [Å] | 87.371, 87.371, 84.662 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 75.670 - 2.300 |
R因子 | 0.177 |
Rwork | 0.174 |
R-free | 0.23000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3gpg |
結合長の平均二乗偏差(RMSD) [Å] | 0.019 |
結合角の平均二乗偏差(RMSD) [度] | 1.774 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0044) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 75.670 | 2.420 |
分解能 [Å] (高) | 2.300 | 2.300 |
独立反射数 | 32115 | |
<I/σ(I)> | 0 | |
完全性 [%] | 100.0 | 100 |
冗長性 | 1 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION | 7.4 | 293 | 46% PEG 600, 100MM HEPES, PH 7.4, VAPOR DIFFUSION, HANGING DROP, TEMPERATURE 293K |