4RR5
The crystal structure of Synechocystis sp. PCC 6803 Malonyl-CoA: ACP Transacylase
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-06-06 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.0000 |
Spacegroup name | P 21 21 2 |
格子定数 [Å] | 43.043, 148.646, 40.393 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 41.345 - 2.427 |
R因子 | 0.1864 |
Rwork | 0.183 |
R-free | 0.25630 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1mla |
結合長の平均二乗偏差(RMSD) [Å] | 0.008 |
結合角の平均二乗偏差(RMSD) [度] | 1.114 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Quality characteristics
Overall | Inner shell | Outer shell | |
分解能 [Å] (低) | 50.000 | 50.000 | 2.660 |
分解能 [Å] (高) | 2.420 | 5.540 | 2.420 |
独立反射数 | 15645 | ||
完全性 [%] | 90.7 | 99.3 | 89.8 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 277 | 0.2M ammonium acetate, 0.1M sodium acetate trihydrate pH 4.6, 30% PEG 4000, VAPOR DIFFUSION, HANGING DROP, temperature 277K |