4PSF
PIH1D1 N-terminal domain
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-11-05 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.92 |
Spacegroup name | P 41 21 2 |
格子定数 [Å] | 60.620, 60.620, 169.990 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 34.798 - 1.578 |
R因子 | 0.1757 |
Rwork | 0.175 |
R-free | 0.19230 |
Structure solution method | MOLECULAR REPLACEMENT |
結合長の平均二乗偏差(RMSD) [Å] | 0.005 |
結合角の平均二乗偏差(RMSD) [度] | 0.960 |
Data reduction software | MOSFLM |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 35.000 | 1.660 |
分解能 [Å] (高) | 1.578 | 1.580 |
独立反射数 | 44722 | |
完全性 [%] | 100.0 | 100 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 291 | 2% PEG 400 (v/v), 20% methoxy PEG 5000, 0.1 M imidazole pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 291K |