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4MYB

Crystal Structure of Francisella tularensis 2-C-methyl-D-erythritol 4-phosphate cytidylyltransferase (IspD)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 14-BM-C
Synchrotron siteAPS
Beamline14-BM-C
Temperature [K]100
Detector technologyCCD
Collection date2011-08-17
DetectorADSC QUANTUM 315
Wavelength(s)0.97870
Spacegroup nameF 41 3 2
Unit cell lengths200.409, 200.409, 200.409
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution30.562 - 2.400
R-factor0.2551
Rwork0.255
R-free0.26560
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.009
RMSD bond angle1.267
Data reduction softwareSAINT
Data scaling softwareSAINT
Phasing softwarePHASER
Refinement softwarePHENIX (1.8_1069)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.5622.580
High resolution limit [Å]2.4002.400
Rmerge0.076
Number of reflections13737
<I/σ(I)>12.358.06
Completeness [%]100.099
Redundancy143
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP4.52950.1 M citric acid, pH 4.5, 7% PEG6000, 0.5 M lithium chloride, VAPOR DIFFUSION, HANGING DROP, temperature 295K

217705

數據於2024-03-27公開中

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