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4MM0

Crystal Structure Analysis of the Putative Thioether Synthase SgvP Involved in the Tailoring Step of Griseoviridin

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRF BEAMLINE BL17U
Synchrotron siteSSRF
BeamlineBL17U
Temperature [K]77.15
Detector technologyCCD
Collection date2012-05-02
DetectorADSC QUANTUM 315
Wavelength(s)0.979228
Spacegroup nameP 41 21 2
Unit cell lengths184.050, 184.050, 80.320
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution29.856 - 2.600
R-factor0.1727
Rwork0.171
R-free0.21380
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2y46
RMSD bond length0.008
RMSD bond angle1.127
Data reduction softwareXDS
Data scaling softwareSCALA
Phasing softwareSOLVE
Refinement softwarePHENIX ((phenix.refine: 1.8.1_1168))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]29.8562.670
High resolution limit [Å]2.6002.600
Number of reflections42958
Completeness [%]99.998.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP8.2277.1520%(w/v) Polyethylene glycol 3350, 0.2M Potassium sodium tartrate tetrahydrate, 3.0%(v/v) Dimethyl sulfoxide, pH 8.2, VAPOR DIFFUSION, SITTING DROP, temperature 277.15K

217705

数据于2024-03-27公开中

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