4L42
Crystal structures of human p70S6K1-PIF
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-09-09 |
Detector | CCD ADSC unsupported-q315 |
Wavelength(s) | 0.9796 |
Spacegroup name | P 65 2 2 |
格子定数 [Å] | 67.656, 67.656, 377.735 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 50.000 - 2.800 |
R因子 | 0.2297 |
Rwork | 0.228 |
R-free | 0.26250 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3a62 |
結合長の平均二乗偏差(RMSD) [Å] | 0.011 |
結合角の平均二乗偏差(RMSD) [度] | 1.529 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0102) |
Quality characteristics
Overall | Inner shell | Outer shell | |
分解能 [Å] (低) | 50.000 | 50.000 | 2.900 |
分解能 [Å] (高) | 2.800 | 6.030 | 2.800 |
Rmerge_l_obs | 0.114 | 0.079 | 0.496 |
独立反射数 | 13601 | ||
<I/σ(I)> | 9.9 | ||
完全性 [%] | 99.3 | 95.6 | 99.9 |
冗長性 | 3.4 | 3 | 3.6 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 6.2 | 289 | 2.0M ammonium sulfate, 0.1M MES, pH 6.2, VAPOR DIFFUSION, HANGING DROP, temperature 289K |