4JCQ
ClpP1 from Listeria monocytogenes
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 140.950, 109.060, 196.260 |
格子定数 [度] | 90.00, 93.16, 90.00 |
精密化法
残基 | 15.000 - 2.000 |
R因子 | 0.19283 |
Rwork | 0.192 |
R-free | 0.21288 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3v5e |
結合長の平均二乗偏差(RMSD) [Å] | 0.005 |
結合角の平均二乗偏差(RMSD) [度] | 0.913 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0117) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 2.100 |
分解能 [Å] (高) | 2.000 | 2.000 |
Rmerge_l_obs | 0.062 | 0.580 |
独立反射数 | 398526 | |
<I/σ(I)> | 16.2 | 3.8 |
完全性 [%] | 99.7 | 99.8 |
冗長性 | 3.4 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 0.1 M Bis-Tris, 0.2 M Li2SO4, 17% PEG3350 , pH 5.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |