4J0U
Crystal structure of IFIT5/ISG58
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-11-15 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.9798 |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 63.722, 71.529, 115.527 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 36.725 - 1.969 |
R因子 | 0.1956 |
Rwork | 0.193 |
R-free | 0.23650 |
Structure solution method | SAD |
結合長の平均二乗偏差(RMSD) [Å] | 0.021 |
結合角の平均二乗偏差(RMSD) [度] | 1.038 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHARP |
Refinement software | PHENIX ((phenix.refine: 1.6.4_486)) |
Quality characteristics
Overall | Inner shell | Outer shell | |
分解能 [Å] (低) | 50.000 | 50.000 | 2.000 |
分解能 [Å] (高) | 1.969 | 5.350 | 1.970 |
独立反射数 | 37930 | ||
完全性 [%] | 99.0 | 98.9 | 100 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 6.9 | 289 | 100mM HEPES, 150mM NaCl, 8% PEG3350, pH 6.9, VAPOR DIFFUSION, HANGING DROP, temperature 289K |
1 | VAPOR DIFFUSION, HANGING DROP | 6.9 | 289 | 100mM HEPES, 150mM NaCl, 8% PEG3350, pH 6.9, VAPOR DIFFUSION, HANGING DROP, temperature 289K |