4GHU
Crystal structure of TRAF3/Cardif
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 77 |
Detector technology | CCD |
Collection date | 2010-01-10 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.000 |
Spacegroup name | P 3 2 1 |
格子定数 [Å] | 83.492, 83.492, 78.125 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 36.819 - 2.199 |
R因子 | 0.1827 |
Rwork | 0.178 |
R-free | 0.22360 |
Structure solution method | MOLECULAR REPLACEMENT |
結合長の平均二乗偏差(RMSD) [Å] | 0.007 |
結合角の平均二乗偏差(RMSD) [度] | 1.042 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MLPHARE |
Refinement software | PHENIX ((phenix.refine: 1.6.4_486)) |
Quality characteristics
Overall | Inner shell | Outer shell | |
分解能 [Å] (低) | 50.000 | 50.000 | 2.240 |
分解能 [Å] (高) | 2.190 | 5.970 | 2.200 |
独立反射数 | 16363 | ||
完全性 [%] | 99.9 | 99.2 | 100 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 289 | 0.1M HEPES, 10% PEG6000, 5%(v/v) 5-methyl-2,4-pentanediol, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 289K |