4D6N
THE CRYSTAL STRUCTURE OF I-DMOI IN COMPLEX WITH ITS TARGET DNA AT 10 DAYS INCUBATION IN 5MM MG (STATE 7)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 106.311, 70.269, 107.169 |
Unit cell angles | 90.00, 119.59, 90.00 |
Refinement procedure
Resolution | 46.598 - 2.350 |
R-factor | 0.1836 |
Rwork | 0.182 |
R-free | 0.21720 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vs8 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.228 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.600 | 2.480 |
High resolution limit [Å] | 2.350 | 2.350 |
Rmerge | 0.070 | 0.460 |
Number of reflections | 56760 | |
<I/σ(I)> | 10.6 | 2.3 |
Completeness [%] | 98.8 | 98.7 |
Redundancy | 3.9 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | pH 5.5 |