4D60
Structure of a dimeric Plasmodium falciparum profilin mutant
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P13 (MX1) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P13 (MX1) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 84.070, 246.460, 256.740 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 19.991 - 3.300 |
R因子 | 0.241 |
Rwork | 0.240 |
R-free | 0.26320 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2jkf |
結合長の平均二乗偏差(RMSD) [Å] | 0.006 |
結合角の平均二乗偏差(RMSD) [度] | 1.129 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 20.000 | 3.390 |
分解能 [Å] (高) | 3.300 | 3.300 |
Rmerge_l_obs | 0.140 | |
独立反射数 | 154448 | |
<I/σ(I)> | 8.1 | 0.7 |
完全性 [%] | 99.6 | 98.3 |
冗長性 | 3.5 | 6.6 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | 6 | 1.8 M AMMONIUM SULFATE, 0.1 M 2-(N- MORPHOLINO)ETHANESULFONIC ACID (PH 6) |