4CWT

Human HSP90 alpha N-terminal domain in complex with an Aminotriazoloquinazoline inhibitor

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2008-05-23
Detector	MAR scanner 345 mm plate
Spacegroup name	I 2 2 2
格子定数 [Å]	67.287, 91.704, 99.275
格子定数 [度]	90.00, 90.00, 90.00

精密化法

残基	30.000 - 1.900
R因子	0.20407
Rwork	0.203
R-free	0.22842
Structure solution method	OTHER
Starting model (for MR)	NONE
結合長の平均二乗偏差(RMSD) [Å]	0.008
結合角の平均二乗偏差(RMSD) [度]	1.406
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	REFMAC (5.6.0117)

Quality characteristics

	Overall	Outer shell
分解能 [Å] (低)	30.000	1.970
分解能 [Å] (高)	1.900	1.900
Rmerge_l_obs	0.060	0.370
独立反射数	24337
<I/σ(I)>	19.8	4.7
完全性 [%]	99.0	97
冗長性	7.2

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1