4CWQ
Human HSP90 alpha N-terminal domain in complex with an Aminotriazoloquinazoline inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2008-01-17 |
Detector | MAR scanner 345 mm plate |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 67.060, 91.007, 98.607 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.000 |
R-factor | 0.19856 |
Rwork | 0.196 |
R-free | 0.24038 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.011 |
RMSD bond angle | 1.321 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.040 | 0.170 |
Number of reflections | 19797 | |
<I/σ(I)> | 17 | 5.8 |
Completeness [%] | 94.8 | 94.6 |
Redundancy | 5.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |