Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

4CU1

Structure of bovine endothelial nitric oxide synthase heme domain in complex with 6-[(2S)-3-amino-2-{5-[2-(6-amino-4-methylpyridin-2-yl)ethyl]pyridin-3-yl}propyl]-4-methylpyridin-2-amine

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 8.2.1
Synchrotron siteALS
Beamline8.2.1
Temperature [K]100
Detector technologyCCD
Collection date2014-02-28
DetectorADSC QUANTUM 315r
Spacegroup nameP 21 21 21
Unit cell lengths57.335, 105.170, 155.044
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution87.040 - 1.890
R-factor0.17143
Rwork0.170
R-free0.20479
Structure solution methodOTHER
Starting model (for MR)NONE
RMSD bond length0.011
RMSD bond angle1.552
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwareREFMAC
Refinement softwareREFMAC (5.8.0049)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.930
High resolution limit [Å]1.9001.900
Rmerge0.0801.000
Number of reflections74481
<I/σ(I)>28.51.2
Completeness [%]99.099.8
Redundancy4.74.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1620-22% PEG3350, 0.1 M CACODYLATE, 150-200 MM MG ACETATE, 5 MM TCEP, pH 6.0

217705

數據於2024-03-27公開中

PDB statisticsPDBj update infoContact PDBjnumon