3ZYB
CRYSTAL STRUCTURE OF PA-IL LECTIN COMPLEXED WITH GALAG0 AT 2.3 A RESOLUTION
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-08-20 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 53.332, 128.559, 146.063 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 49.261 - 2.290 |
R因子 | 0.2151 |
Rwork | 0.214 |
R-free | 0.24040 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1l7l |
結合長の平均二乗偏差(RMSD) [Å] | 0.002 |
結合角の平均二乗偏差(RMSD) [度] | 0.691 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 73.070 | 2.430 |
分解能 [Å] (高) | 2.290 | 2.290 |
Rmerge_l_obs | 0.100 | 0.440 |
独立反射数 | 45434 | |
<I/σ(I)> | 10 | 2.8 |
完全性 [%] | 98.8 | 93.5 |
冗長性 | 3.63 | 3.5 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | 3.5 | 0.1 M CITRIC ACID PH 3.5 AND 25% W/V POLYETHYLENE GLYCOL 3350 |