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3ZCW

Eg5 - New allosteric binding site

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I02
Synchrotron siteDiamond
BeamlineI02
Temperature [K]100
Detector technologyCCD
Collection date2011-09-18
DetectorADSC QUANTUM 315r
Spacegroup nameC 1 2 1
Unit cell lengths107.940, 62.890, 75.050
Unit cell angles90.00, 117.46, 90.00
Refinement procedure
Resolution28.468 - 1.691
R-factor0.196
Rwork0.194
R-free0.23280
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2wog
RMSD bond length0.011
RMSD bond angle1.414
Data reduction softwareXDS
Data scaling softwareSCALA
Phasing softwareMOLREP
Refinement softwarePHENIX ((PHENIX.REFINE))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]36.9601.780
High resolution limit [Å]1.6901.690
Rmerge0.0800.660
Number of reflections49475
<I/σ(I)>9.32
Completeness [%]99.299.2
Redundancy3.93.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
16.920% PEG3350, 2MM MAGNESIUM CHLORIDE, 100MM HEPES PH 7.5

217705

건을2024-03-27부터공개중

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