3TV0
Structure of dynactin p27 subunit
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-06-27 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 1 |
Spacegroup name | C 1 2 1 |
格子定数 [Å] | 84.960, 57.140, 80.190 |
格子定数 [度] | 90.00, 108.50, 90.00 |
精密化法
残基 | 43.451 - 2.149 |
R因子 | 0.2163 |
Rwork | 0.214 |
R-free | 0.25790 |
Structure solution method | MOLECULAR REPLACEMENT |
結合長の平均二乗偏差(RMSD) [Å] | 0.008 |
結合角の平均二乗偏差(RMSD) [度] | 1.144 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | BALBES |
Refinement software | PHENIX ((phenix.refine: 1.6.4_486)) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 43.500 | 2.190 |
分解能 [Å] (高) | 2.149 | 2.149 |
独立反射数 | 16255 | |
完全性 [%] | 81.1 | 38.4 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION | 3.6 | 295 | 19% PEG 2000, 0.15 M Potassium phosphate, pH 3.6, VAPOR DIFFUSION, temperature 295K |