3T7J
Crystal structure of Rtt107p (residues 820-1070)
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-03-24 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.9790 |
Spacegroup name | P 1 |
格子定数 [Å] | 34.357, 62.182, 65.801 |
格子定数 [度] | 86.64, 75.38, 73.98 |
精密化法
残基 | 32.052 - 2.042 |
R因子 | 0.2058 |
Rwork | 0.203 |
R-free | 0.25380 |
Structure solution method | MOLECULAR REPLACEMENT |
結合長の平均二乗偏差(RMSD) [Å] | 0.007 |
結合角の平均二乗偏差(RMSD) [度] | 1.060 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER (2.2.4) |
Refinement software | PHENIX (1.6.1_357) |
Quality characteristics
Overall | Inner shell | Outer shell | |
分解能 [Å] (低) | 50.000 | 50.000 | 2.080 |
分解能 [Å] (高) | 2.040 | 5.540 | 2.040 |
Rmerge_l_obs | 0.059 | 0.042 | 0.206 |
独立反射数 | 31394 | ||
<I/σ(I)> | 19.7 | ||
完全性 [%] | 96.5 | 93.4 | 83.1 |
冗長性 | 3.8 | 3.7 | 3.5 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 283 | 20%(w/v) MPEG2000, 0.2M NaCl, 0.1M HEPES, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 283K |