3QKS
Mre11 Rad50 binding domain bound to Rad50
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-05-01 |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 55.779, 91.232, 107.331 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.670 - 2.100 |
R-factor | 0.2125 |
Rwork | 0.210 |
R-free | 0.25610 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ii8 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.679 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | PHENIX ((phenix.refine: 1.6.1_357)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.670 | 2.168 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.051 | 0.457 |
Number of reflections | 31661 | |
<I/σ(I)> | 27.5 | 2.8 |
Completeness [%] | 96.8 | 86 |
Redundancy | 4.6 | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | 100 mM Tris, 200 mM magnesium chloride, 20% PEG3350, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |