3MSE
Crystal structure of C-terminal domain of PF110239.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-03-24 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9792 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 101.757, 101.757, 44.895 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 50.000 - 2.100 |
R-factor | 0.224 |
Rwork | 0.222 |
R-free | 0.26400 |
Structure solution method | SAD |
RMSD bond length | 0.011 |
RMSD bond angle | 1.139 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHELXS |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.140 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.074 | 0.691 |
Number of reflections | 15859 | |
<I/σ(I)> | 9.9 | 4.55 |
Completeness [%] | 99.8 | 100 |
Redundancy | 11.1 | 11.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 30 % PEG 400, 0.2 M Ammonium sulfate, 0.05 M Hepes 7.5, 2 mM AMPPNP, 4 mM CaCL2, MgCl2, 6.25 mM TCEp, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 30 % PEG 400, 0.2 M Ammonium sulfate, 0.05 M Hepes 7.5, 2 mM AMPPNP, 4 mM CaCL2, MgCl2, 6.25 mM TCEp, VAPOR DIFFUSION, HANGING DROP, temperature 293K |