3M0A
Crystal structure of TRAF2:cIAP2 complex
Experimental procedure
実験手法 | MAD |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X25 |
Synchrotron site | NSLS |
Beamline | X25 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-03-28 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.2822,1.2832,1.2664 |
Spacegroup name | I 41 |
格子定数 [Å] | 92.123, 92.123, 85.971 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 32.600 - 2.610 |
Rwork | 0.227 |
R-free | 0.26800 |
Structure solution method | MAD |
結合長の平均二乗偏差(RMSD) [Å] | 0.019 |
結合角の平均二乗偏差(RMSD) [度] | 1.878 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | REFMAC (5.5.0072) |
Quality characteristics
Overall | Inner shell | Outer shell | |
分解能 [Å] (低) | 50.000 | 50.000 | 2.690 |
分解能 [Å] (高) | 2.600 | 5.600 | 2.600 |
Rmerge_l_obs | 0.049 | 0.028 | 0.393 |
独立反射数 | 11032 | ||
<I/σ(I)> | 15.8 | ||
完全性 [%] | 88.7 | 95.3 | 46.4 |
冗長性 | 3.6 | 3.6 | 2.5 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 293 | 8% PEG 3350, 6% Tacsimate, pH 5.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |