3LQZ
Crystal Structure of HLA-DP2
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Temperature [K] | 170 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0 |
Spacegroup name | P 31 2 1 |
格子定数 [Å] | 157.282, 157.282, 61.805 |
格子定数 [度] | 90.00, 90.00, 120.00 |
精密化法
残基 | 50.000 - 3.250 |
R因子 | 0.21865 |
Rwork | 0.217 |
R-free | 0.25094 |
Structure solution method | MOLECULAR REPLACEMENT |
結合長の平均二乗偏差(RMSD) [Å] | 0.012 |
結合角の平均二乗偏差(RMSD) [度] | 1.490 |
Data reduction software | HKL-2000 |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.3.0040) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 136.080 | 3.283 |
分解能 [Å] (高) | 3.250 | 3.250 |
独立反射数 | 12053 | |
完全性 [%] | 100.0 | 89.1 |
冗長性 | 7.1 | 6 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 20% PEG4000, 300mM Sodium Chloride, HEPES, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 20% PEG4000, 300mM Sodium Chloride, HEPES, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |