Experimental procedure
| 実験手法 | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU FR-E SUPERBRIGHT |
| Temperature [K] | 95 |
| Detector technology | IMAGE PLATE |
| Collection date | 2005-05-27 |
| Detector | RIGAKU RAXIS HTC |
| Wavelength(s) | 1.54182 |
| Spacegroup name | P 21 21 21 |
| 格子定数 [Å] | 85.440, 88.840, 105.390 |
| 格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
| 残基 | 67.420 - 2.100 |
| R因子 | 0.2226 |
| Rwork | 0.220 |
| R-free | 0.26480 |
| Structure solution method | FOURIER SYNTHESIS |
| 結合長の平均二乗偏差(RMSD) [Å] | 0.011 |
| 結合角の平均二乗偏差(RMSD) [度] | 1.208 |
| Data reduction software | CrystalClear |
| Data scaling software | CrystalClear |
| Phasing software | BUSTER-TNT (1.3.1) |
| Refinement software | BUSTER-TNT (1.3.1) |
Quality characteristics
| Overall | Outer shell | |
| 分解能 [Å] (低) | 100.000 | 2.180 |
| 分解能 [Å] (高) | 2.100 | 2.100 |
| Rmerge_l_obs | 0.044 | 0.469 |
| 独立反射数 | 46716 | |
| <I/σ(I)> | 11.6 | 2.2 |
| 完全性 [%] | 98.2 | 98.1 |
| 冗長性 | 3.68 | 3.66 |
結晶化条件
| 結晶ID | 方法 | pH | 温度 | 溶液条件 |
| 1 | VAPOR DIFFUSION | 7 | 277 | 10-30% MPD OR ISOPROPANOL, 100 mM IMIDAZOLE, 1 mM SR12813, pH 7, VAPOR DIFFUSION, temperature 277K |
