3HMG

REFINEMENT OF THE INFLUENZA VIRUS HEMAGGLUTININ BY SIMULATED ANNEALING

Experimental procedure

Spacegroup name	P 41
Unit cell lengths	162.800, 162.800, 177.300
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	? - 2.900
Rwork	0.238
RMSD bond length	0.015
RMSD bond angle	27.000 *
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	12.000 *
High resolution limit [Å]	2.900 *
Rmerge	0.126 *
Number of reflections	74683 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Microdialysis *			referred to 'Weis, W.', (1988) Nature, 333, 426-431 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	protein	35 (mg/ml)
2	1	2	Na3 citrate	1.34-1.38 (%sat)
3	1	2		0.1 (%)