3H7G
Apo-FR with AU ions
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL38B1 |
Synchrotron site | SPring-8 |
Beamline | BL38B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2007-03-08 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 1.0395 |
Spacegroup name | F 4 3 2 |
Unit cell lengths | 181.632, 181.632, 181.632 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.280 - 1.650 |
R-factor | 0.21 |
Rwork | 0.209 |
R-free | 0.23600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1dat |
RMSD bond length | 0.008 |
RMSD bond angle | 1.105 |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.000 | 1.710 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.082 | 0.309 |
Number of reflections | 31508 | |
<I/σ(I)> | 67.8 | 8.01 |
Completeness [%] | 100.0 | 100 |
Redundancy | 20.2 | 14 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | AMMONIUM SULFATE, CADMIUM SULFATE, VAPOR DIFFUSION, HANGING DROP, temperature 293K | |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | AMMONIUM SULFATE, CADMIUM SULFATE, VAPOR DIFFUSION, HANGING DROP, temperature 293K |