3EYJ
Structure of Influenza Haemagglutinin in complex with an inhibitor of membrane fusion
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2006-10-10 |
Detector | RIGAKU RAXIS IIC |
Wavelength(s) | 1.54 |
Spacegroup name | P 21 3 |
Unit cell lengths | 138.765, 138.765, 138.765 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.585 - 2.600 |
R-factor | 0.1959 |
Rwork | 0.193 |
R-free | 0.24450 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | PHENIX ((phenix.refine)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 27461 | |
Completeness [%] | 99.5 | 99.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | Tris, PEG8000, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |