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3DJU

Crystal structure of human BTG2

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-5A
Synchrotron sitePhoton Factory
BeamlineBL-5A
Temperature [K]100
Detector technologyCCD
Collection date2008-01-27
DetectorADSC QUANTUM 315
Wavelength(s)1.0000
Spacegroup nameP 21 21 21
Unit cell lengths39.272, 40.751, 67.971
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution34.940 - 2.260
R-factor0.19759
Rwork0.194
R-free0.26341
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2d5r
RMSD bond length0.014
RMSD bond angle1.452
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 Overall
Low resolution limit [Å]50.000
High resolution limit [Å]2.260
Rmerge0.057
Number of reflections5309
Redundancy4.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.1289100mM BIS-TRIS, 0.2M Sodium chloride, 21% (v/v) PEG 3350, pH 6.1, VAPOR DIFFUSION, HANGING DROP, temperature 289K

217705

數據於2024-03-27公開中

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