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3CEQ

The TPR domain of Human Kinesin Light Chain 2 (hKLC2)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 23-ID-B
Synchrotron siteAPS
Beamline23-ID-B
Collection date2007-07-07
Wavelength(s).979
Spacegroup nameP 21 21 21
Unit cell lengths70.422, 99.940, 103.106
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution30.000 - 2.750
R-factor0.236
Rwork0.234
R-free0.27100
Structure solution methodSAD
RMSD bond length0.006
RMSD bond angle0.845
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareSOLVE
Refinement softwareREFMAC (refmac_5.2.0019)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]50.00050.0002.690
High resolution limit [Å]2.6005.6002.600
Rmerge0.1440.0700.583
Number of reflections21563
<I/σ(I)>16.5
Completeness [%]94.399.868.8
Redundancy13.3164.2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6.62931.46 M Ammonium Sulfate, 0.2 M Sodium Acetate, 0.1 M Bis-Tris pH 6.6, VAPOR DIFFUSION, SITTING DROP, temperature 293K

217705

数据于2024-03-27公开中

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