3C5J
Crystal structure of HLA DR52c
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-11-11 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979 |
Spacegroup name | P 43 2 2 |
格子定数 [Å] | 83.380, 83.380, 132.910 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 41.690 - 1.800 |
Rwork | 0.202 |
R-free | 0.22700 |
結合長の平均二乗偏差(RMSD) [Å] | 0.005 |
結合角の平均二乗偏差(RMSD) [度] | 1.300 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 1.860 |
分解能 [Å] (高) | 1.800 | 1.800 |
Rmerge_l_obs | 0.064 | 0.803 |
独立反射数 | 42787 | |
<I/σ(I)> | 14.9 | 2.1 |
完全性 [%] | 96.5 | 87.7 |
冗長性 | 5.7 | 4.6 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | 1.6 M ammonium sulfate, pH 7.5, vapor diffusion, hanging drop, temperature 298K |