3BY2

Norwalk P polypeptide (228-523)

Experimental procedure

実験手法	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RUH3R
Temperature [K]	100
Detector technology	IMAGE PLATE
Detector	RIGAKU RAXIS IV++
Wavelength(s)	1.5418
Spacegroup name	I 21 21 21
格子定数 [Å]	82.799, 83.771, 102.229
格子定数 [度]	90.00, 90.00, 90.00

精密化法

残基	50.000 - 2.600
Rwork	0.212
R-free	0.27080
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1ihm
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	CNS
Refinement software	CNS

Quality characteristics

	Overall
分解能 [Å] (低)	50.000
分解能 [Å] (高)	2.600
独立反射数	8083
冗長性	1.9

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1