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3AWD

Crystal structure of gox2181

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsNSLS BEAMLINE X29A
Synchrotron siteNSLS
BeamlineX29A
Temperature [K]100
Detector technologyCCD
Collection date2010-06-30
DetectorADSC QUANTUM 315
Wavelength(s)1.075
Spacegroup nameP 21 21 21
Unit cell lengths63.273, 121.416, 136.546
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution50.000 - 1.800
R-factor0.15224
Rwork0.151
R-free0.18448
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.012
RMSD bond angle1.189
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASES
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]90.9101.830
High resolution limit [Å]1.8001.800
Rmerge0.0950.503
Number of reflections92746
<I/σ(I)>24.34.03
Completeness [%]99.699.9
Redundancy7.36.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.1293PEG 8K MG, HEPES, pH 7.1, VAPOR DIFFUSION, HANGING DROP, temperature 293K

217705

數據於2024-03-27公開中

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