3A64
Crystal structure of CcCel6C, a glycoside hydrolase family 6 enzyme, from Coprinopsis cinerea
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
Synchrotron site | Photon Factory |
Beamline | AR-NW12A |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-03-09 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 |
格子定数 [Å] | 44.035, 45.112, 48.904 |
格子定数 [度] | 77.81, 87.34, 68.79 |
精密化法
残基 | 19.080 - 1.600 |
R因子 | 0.14309 |
Rwork | 0.141 |
R-free | 0.16541 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1bvw |
結合長の平均二乗偏差(RMSD) [Å] | 0.008 |
結合角の平均二乗偏差(RMSD) [度] | 1.117 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 1.660 |
分解能 [Å] (高) | 1.598 | 1.598 |
Rmerge_l_obs | 0.025 | 0.090 |
独立反射数 | 43370 | |
<I/σ(I)> | 33.2 | 9.21 |
完全性 [%] | 95.8 | 94 |
冗長性 | 2 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 30% PEG 8000, 0.1M HEPES-KOH, 0.15M magnesium acetate, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |