2Z6T
Crystal structure of the ferric peroxo myoglobin
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44B2 |
Synchrotron site | SPring-8 |
Beamline | BL44B2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-12-15 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.6 |
Spacegroup name | P 1 21 1 |
格子定数 [Å] | 34.336, 30.706, 63.682 |
格子定数 [度] | 90.00, 105.44, 90.00 |
精密化法
残基 | 8.000 - 1.200 |
R因子 | 0.131 |
Rwork | 0.131 |
R-free | 0.18500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2z6s |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNS |
Refinement software | CNS |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 50.000 | 1.240 |
分解能 [Å] (高) | 1.200 | 1.200 |
独立反射数 | 39884 | |
<I/σ(I)> | 27.8 | 2.78 |
完全性 [%] | 99.0 | |
冗長性 | 3.5 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | LIQUID DIFFUSION | 6 | 293 | Ammonium Sulfate, pH6.0, LIQUID DIFFUSION, temperature 293K |