2Y1L
Caspase-8 in Complex with DARPin-8.4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 90 |
Detector technology | PIXEL |
Collection date | 2010-04-23 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 61.000, 81.600, 163.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.857 - 1.800 |
R-factor | 0.182 |
Rwork | 0.180 |
R-free | 0.21780 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ENTRIES 1QDU AND 2QYJ |
RMSD bond length | 0.009 |
RMSD bond angle | 1.201 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.860 | 1.850 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.100 | 0.510 |
Number of reflections | 75862 | |
<I/σ(I)> | 13.29 | 3.76 |
Completeness [%] | 99.4 | 98.9 |
Redundancy | 4.9 | 4.88 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.8 | 100 MM CITRIC ACID PH 4.9 (RT), 200 MM LI2SO4, 22.5% PEG 4K. |