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2XTE

Structure of the TBL1 tetramerisation domain

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I04
Synchrotron siteDiamond
BeamlineI04
Temperature [K]100
Detector technologyCCD
Collection date2008-06-22
DetectorADSC CCD
Spacegroup nameP 21 21 21
Unit cell lengths88.020, 150.190, 164.830
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution111.100 - 3.900
R-factor0.273
Rwork0.273
R-free0.30200
Structure solution methodMIR
Starting model (for MR)2xtc
RMSD bond length0.011
RMSD bond angle1.240
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwareCNS (1.2)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]111.1004.110
High resolution limit [Å]3.9003.900
Rmerge0.1100.320
Number of reflections19503
<I/σ(I)>9.14
Completeness [%]99.9100
Redundancy3.53.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
16.50.1 M MES PH6.5, 2.0 M NACL, 0.175 M SODIUM ACETATE, 19 % GLYCEROL

217705

数据于2024-03-27公开中

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