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2XTC

Structure of the TBL1 tetramerisation domain

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I03
Synchrotron siteDiamond
BeamlineI03
Temperature [K]100
Detector technologyCCD
Collection date2008-12-13
DetectorADSC CCD
Spacegroup nameP 61 2 2
Unit cell lengths59.541, 59.541, 193.880
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution51.570 - 2.220
R-factor0.23854
Rwork0.237
R-free0.26437
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1uuj
RMSD bond length0.015
RMSD bond angle1.494
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]96.0002.320
High resolution limit [Å]2.2002.200
Rmerge0.0700.400
Number of reflections10905
<I/σ(I)>15.13.9
Completeness [%]99.9100
Redundancy6.56.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
17.417% PEG 4000, 0.2 M MGCL2, 0.1 M TRIS/HCL PH8.5, pH 7.4

217705

数据于2024-03-27公开中

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