2XSM
Crystal structure of the mammalian cytosolic chaperonin CCT in complex with tubulin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2008-10-15 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 272.700, 313.500, 158.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 100.000 - 5.500 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | REFMAC (5.5.0099) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 6.000 |
High resolution limit [Å] | 5.500 | 5.500 |
Rmerge | 0.050 | 0.650 |
Number of reflections | 74325 | |
<I/σ(I)> | 9.54 | 1.2 |
Completeness [%] | 92.5 | 95.3 |
Redundancy | 4.1 | 3.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | 1 M LICL, 100 MM MES PH 6, 10% PEG6000, 10% OF THE OPTIC SALT SUITE NUMBER 63 FROM QIAGEN, AND 5% OF TERT-BUTANOL FROM HAMPTON RESEARCH ADDITIVE SCREEN. |