2XD4
Nucleotide-bound Structures of Bacillus subtilis Glycinamide Ribonucleotide Synthetase
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1998-10-28 |
Detector | RIGAKU RAXIS-IIC |
Spacegroup name | P 21 21 21 |
格子定数 [Å] | 56.990, 84.410, 85.720 |
格子定数 [度] | 90.00, 90.00, 90.00 |
精密化法
残基 | 38.220 - 2.650 |
R因子 | 0.207 |
Rwork | 0.204 |
R-free | 0.27000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2xcl |
結合長の平均二乗偏差(RMSD) [Å] | 0.006 |
結合角の平均二乗偏差(RMSD) [度] | 0.900 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNX (2005) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 38.210 | 2.740 |
分解能 [Å] (高) | 2.650 | 2.650 |
Rmerge_l_obs | 0.100 | 0.220 |
独立反射数 | 11710 | |
<I/σ(I)> | 22.6 | |
完全性 [%] | 93.4 | 66.4 |
冗長性 | 4 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | 7.5 | 30% PEG 4000, 0.1 M TRIS-HCL PH 8.5, 4.2 MM MGCL2, 1.8 MM ATP |