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2X9C

Crystal structure of a soluble PrgI mutant from Salmonella Typhimurium

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID23-1
Synchrotron siteESRF
BeamlineID23-1
Temperature [K]100
Detector technologyCCD
Collection date2007-05-13
DetectorADSC QUANTUM 315r
Spacegroup nameP 31 1 2
Unit cell lengths64.530, 64.530, 104.290
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution38.130 - 2.450
R-factor0.225
Rwork0.225
R-free0.23900
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2ca5
RMSD bond length0.008
RMSD bond angle1.100
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHASER
Refinement softwareCNS (1.21)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.310
High resolution limit [Å]2.2502.250
Rmerge0.1100.920
Number of reflections11435
<I/σ(I)>9.832.11
Completeness [%]94.996.8
Redundancy7.57.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROPRESERVOIR SOLUTION 0.15 MM NAH2PO4. SAMPLE BUFFER 20 MM HEPES (PH 7.5) 50 MM NACL. HANGING DROP WITH 1 UL SAMPLE AND 1 UL RESERVOIR SOLUTION.

217705

數據於2024-03-27公開中

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