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2WXF

The crystal structure of the murine class IA PI 3-kinase p110delta in complex with PIK-39.

Experimental procedure
実験手法SINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE ID14-2
Synchrotron siteESRF
BeamlineID14-2
Temperature [K]100
Detector technologyCCD
Collection date2008-07-20
DetectorADSC CCD
Spacegroup nameC 1 2 1
格子定数 [Å]142.420, 65.010, 116.690
格子定数 [度]90.00, 103.53, 90.00
精密化法
残基38.950 - 1.900
R因子0.21052
Rwork0.210
R-free0.23986
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2rd0
結合長の平均二乗偏差(RMSD) [Å]0.012
結合角の平均二乗偏差(RMSD) [度]1.253
Data reduction softwareiMOSFLM
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwareREFMAC (5.5.0046)
Quality characteristics
 OverallOuter shell
分解能 [Å] (低)38.9501.920
分解能 [Å] (高)1.9001.900
Rmerge_l_obs0.0700.840
独立反射数80511
<I/σ(I)>16.311.78
完全性 [%]98.596.3
冗長性6.796.77
結晶化条件
結晶ID方法pH温度溶液条件
16.820% (V/V) GLYCEROL, 10% (W/V) PEG 4K, 30 MM NANO3, 30 MM NA2HPO4, 30 MM (NH4)2SO4, 100 MM IMIDAZOLE PH 6.8

217705

件を2024-03-27に公開中

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