2WIH
STRUCTURE OF CDK2-CYCLIN A WITH PHA-848125
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-04-28 |
Detector | ADSC CCD |
Spacegroup name | P 62 2 2 |
Unit cell lengths | 183.000, 183.000, 213.560 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.960 - 2.500 |
R-factor | 0.215 |
Rwork | 0.213 |
R-free | 0.25000 |
Structure solution method | OTHER |
Starting model (for MR) | NONE |
RMSD bond length | 0.006 |
RMSD bond angle | 0.900 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | CNX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.600 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.090 | 0.570 |
Number of reflections | 72932 | |
<I/σ(I)> | 16.1 | 3.7 |
Completeness [%] | 99.7 | 100 |
Redundancy | 7 | 0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 20% AMMONIUM SULPHATE, 1M KCL, 40MM HEPES PH 7 |