2WFE
Structure of the Candida albicans cytosolic leucyl-tRNA synthetase editing domain
Experimental procedure
実験手法 | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 1 2 1 |
格子定数 [Å] | 101.060, 43.040, 122.170 |
格子定数 [度] | 90.00, 107.57, 90.00 |
精密化法
残基 | 28.830 - 2.900 |
R因子 | 0.24457 |
Rwork | 0.241 |
R-free | 0.30085 |
Structure solution method | MOLECULAR REPLACEMENT |
結合長の平均二乗偏差(RMSD) [Å] | 0.007 |
結合角の平均二乗偏差(RMSD) [度] | 1.023 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.5.0070) |
Quality characteristics
Overall | Outer shell | |
分解能 [Å] (低) | 30.000 | 3.020 |
分解能 [Å] (高) | 2.900 | 2.900 |
Rmerge_l_obs | 0.150 | 0.400 |
独立反射数 | 21666 | |
<I/σ(I)> | 8.55 | 2.92 |
完全性 [%] | 94.8 | 71.5 |
冗長性 | 3 | 1.77 |
結晶化条件
結晶ID | 方法 | pH | 温度 | 溶液条件 |
1 | 0.2 M AMMONIUM ACETATE, 0.01 M MAGNESIUM ACETATE TETRAHYDRATE, 0.05 M SODIUM CACODYLATE TRIHYDRATE PH 6.5, 30% W/V POLYETHYLENE GLYCOL 8000 |